This paper presents a definitive synthetic proof of the impossibility of trisecting an arbitrary angle within Euclidean geometry. The proof centers not on algebraic abstractions, but on an intrinsic geometric inconsistency revealed through the lens of the canonical 90° angle. This angle serves not merely as a counterexample, but as a diagnostic lever that fractures the very concept of a universal trisection property. A new “Principle of Operational Dissonance” is formulated from an analysis of foundational operations, such as doubling and cubing a square’s diagonal. These operations, while producing congruent final magnitudes, violate the core Euclidean doctrine of proportional similarity, demonstrating that (a:b ≠ c:d) in a strict geometric sense. This dissonance mirrors the logical structure of the trisection problem. The proof demonstrates that assuming the existence of a universal trisection procedure forces a specific geometric condition-the equality of certain lengths-when applied to a 90° angle. This condition arises solely from the angle’s axiomatic status and the constraints of compass-and-straightedge constructions. However, this forced condition is not preserved under variation of the angle measure, rendering any purported universal procedure internally inconsistent. The resulting contradiction proves the impossibility of trisecting a 90° angle with a universal method. This failure, stemming from a fundamental incompatibility within the geometric system rather than the peculiarities of a single angle, extends to all angles, conclusively resolving the classical problem. The proof thus delineates the exact boundary of classical constructive geometry, indicating that any future universal solution must arise from the introduction of new geometric properties innately compatible with Euclidean theory. It reaffirms the self-contained sufficiency of Euclidean geometry for resolving its celebrated problems and challenges the methodological necessity of importing non-geometric techniques to establish geometric impossibilities. The presented framework offers a purely synthetic geometric perspective, one that aligns with the foundational spirit of Euclid’s Elements.