Preprint Article Version 1 Preserved in Portico This version is not peer-reviewed

Fast Bimetallic Nanoalloy Quantification Method Using X-ray Fluorescence Spectroscopy for High-Throughput Experiments

Version 1 : Received: 22 November 2023 / Approved: 23 November 2023 / Online: 23 November 2023 (03:37:14 CET)

How to cite: Nguyen-Vu, L. Fast Bimetallic Nanoalloy Quantification Method Using X-ray Fluorescence Spectroscopy for High-Throughput Experiments. Preprints 2023, 2023111452. https://doi.org/10.20944/preprints202311.1452.v1 Nguyen-Vu, L. Fast Bimetallic Nanoalloy Quantification Method Using X-ray Fluorescence Spectroscopy for High-Throughput Experiments. Preprints 2023, 2023111452. https://doi.org/10.20944/preprints202311.1452.v1

Abstract

High-throughput research on bimetallic nanoparticles brought a vast overview of their characteristics and catalytic activities.1 However, traditional bimetallic nano-allloy quantification methods serving catalyst preparations are not suitable for the fast and robust data output of high-throughput experiments. Hence, this work designed and validated a more fast, more neat, and reliable quantitative analysis using X-ray fluorescence spectroscopy for bimetallic nanoparticles synthesized by high-throughput setups. The results demonstrated this method to be accurate with high precision. Furthermore, the agreement to qualitative results from an energy-dispersive X-ray spectrometer equiped on a scanning electron microscope provided an option to quantify a bimetallic nano-alloy by just analyzing one of the two composing elements. Thus, this method is proved to be highly compatible with high-throughput experiments.

Keywords

quantitative analysis; X-ray fluorescence spectroscopy; bimetallic nanoparticle; nanoparticle concentration

Subject

Chemistry and Materials Science, Analytical Chemistry

Comments (0)

We encourage comments and feedback from a broad range of readers. See criteria for comments and our Diversity statement.

Leave a public comment
Send a private comment to the author(s)
* All users must log in before leaving a comment
Views 0
Downloads 0
Comments 0
Metrics 0


×
Alerts
Notify me about updates to this article or when a peer-reviewed version is published.
We use cookies on our website to ensure you get the best experience.
Read more about our cookies here.