Preprint Article Version 1 Preserved in Portico This version is not peer-reviewed

Fabrication of Gold-Graphitic Carbon Nitride Composite Electrode for the Detection of Pimobendan

Version 1 : Received: 25 June 2023 / Approved: 26 June 2023 / Online: 26 June 2023 (05:32:37 CEST)

How to cite: Luk, H.; Chang, X.; Wu, R. Fabrication of Gold-Graphitic Carbon Nitride Composite Electrode for the Detection of Pimobendan. Preprints 2023, 2023061748. https://doi.org/10.20944/preprints202306.1748.v1 Luk, H.; Chang, X.; Wu, R. Fabrication of Gold-Graphitic Carbon Nitride Composite Electrode for the Detection of Pimobendan. Preprints 2023, 2023061748. https://doi.org/10.20944/preprints202306.1748.v1

Abstract

In this study, the preparation of the composite 3% Au/graphite-C3N4 (3% Au/g-C3N4) sensing material was prepared by doping 3% Au onto the surface of graphitic carbonitride (C3N4) for detection pimobendan. By the way of sensing materials characterization, the X-ray diffraction analysis (XRD) and transmission electron Microscope (TEM) were performed. The cyclic voltammetry (CV) was used to measure the concentration and redox properties of pimobendan. It can be seen that when the voltage value is 0.05 V, and a reduction peak was appeared and the pimobendan concentration (0 to 55 μM) has a relationship with the reduction current value. At low concentrations of pimobendan concentration from 0.0 to 0.8 μM, the linearity R2 = 0.9642 with a detection limit of 0.28 μM. A possible pimobendan sensing mechanism on 3% Au/g-C3N4 was proposed.

Keywords

electrochemical; sensor; Au/g-C3N4; pimobendan

Subject

Chemistry and Materials Science, Electrochemistry

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