Preprint Article Version 1 Preserved in Portico This version is not peer-reviewed

Realization of Phase and Microstructure Control in Fe/Fe2SiO4-FeAl2O4 Metal-Ceramic by Alternative Microwave Susceptors

Version 1 : Received: 4 January 2022 / Approved: 6 January 2022 / Online: 6 January 2022 (09:42:02 CET)

A peer-reviewed article of this Preprint also exists.

Gao, C.; Xu, P.; Ruan, F.; Yang, C. Realization of Phase and Microstructure Control in Fe/Fe2SiO4-FeAl2O4 Metal–Ceramic by Alternative Microwave Susceptors. Materials 2022, 15, 1905. Gao, C.; Xu, P.; Ruan, F.; Yang, C. Realization of Phase and Microstructure Control in Fe/Fe2SiO4-FeAl2O4 Metal–Ceramic by Alternative Microwave Susceptors. Materials 2022, 15, 1905.

Abstract

This study provides a novel method to prepare metal-ceramic composites from magnetically selected iron ore using microwave heating. By introducing three different microwave susceptors (Activated Carbon, SiC, and a mixture of Activated Carbon and SiC) during the microwave process, effective control of the ratio of metallic and ceramic phases has been achieved easily. The effects of the three susceptors on the microstructure of the metal-ceramics and the related reaction mechanisms were also investigated in detail. The results show that the metal phase (Fe) and ceramic phase (Fe2SiO4, FeAl2O4) can be maintained, but the metal phase to ceramic phase changed significantly. In particular, the microstructures appeared as well-distributed nanosheet structures with diameters of ~400 nm and thicknesses of ~20 nm when SiC was used as the microwave susceptor.

Keywords

metal-ceramic; microwave sintering; susceptor; phase modulation; nanostructures

Subject

Chemistry and Materials Science, Metals, Alloys and Metallurgy

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