Preprint Article Version 1 Preserved in Portico This version is not peer-reviewed

Synergistic Improvement of Mechanical and Corrosion Properties in TiN PVD-Coated Tool Steels via PAN Pre-treatment

Version 1 : Received: 28 September 2023 / Approved: 28 September 2023 / Online: 29 September 2023 (04:08:21 CEST)

How to cite: Dadfar, M.; Khandan Pour, H.R.; Sanvito, T. Synergistic Improvement of Mechanical and Corrosion Properties in TiN PVD-Coated Tool Steels via PAN Pre-treatment. Preprints 2023, 2023092019. https://doi.org/10.20944/preprints202309.2019.v1 Dadfar, M.; Khandan Pour, H.R.; Sanvito, T. Synergistic Improvement of Mechanical and Corrosion Properties in TiN PVD-Coated Tool Steels via PAN Pre-treatment. Preprints 2023, 2023092019. https://doi.org/10.20944/preprints202309.2019.v1

Abstract

Chemical and mechanical properties of plasma-assisted nitrided (PAN), TiN cathodic arc coated, and PAN with TiN coated samples were thoroughly evaluated on tool steel samples of 1.2379. The evaluation involved SEM, nano-indentation, profilometer, micro scratch, and corrosion tests. The results revealed that PAN treatment alters the roughness of the surface, while it has minimal impact on the coefficient of friction. However, it increases the substrate's hardness, making it twice as hard and three times more resilient against scratch tests, along with improved corrosion resistance. TiN-coated samples are four times harder than untreated ones, but they exhibit a higher elastic modulus (E), leading to a lower H/E index. The most promising results were obtained with PAN+TiN treatment, combining high hardness (H) with lower E, resulting in a high H/E index, a crucial criterion for wear resistance. These samples also demonstrated superior scratch hardness and corrosion resistance, despite being thinner and rougher.

Keywords

nitriding; physical vapour deposition (PVD); mechanical properties testing; corrosion; scratch hardness

Subject

Engineering, Metallurgy and Metallurgical Engineering

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