Preprint Article Version 1 Preserved in Portico This version is not peer-reviewed

Testing of a Prototype Combining Ultrasound and Pulsed Electric Field on Extracted Valuable Compounds of Mitragyna speciosa Leaves

Version 1 : Received: 11 July 2023 / Approved: 12 July 2023 / Online: 13 July 2023 (05:06:28 CEST)

A peer-reviewed article of this Preprint also exists.

Jintawiwat, R.; Punamorntarakul, N.; Hirunyasiri, R.; Jarupoom, P.; Pankasemsuk, T.; Supasin, S.; Kawee-ai, A. Testing the Efficacy of a Prototype That Combines Ultrasound and Pulsed Electric Field for Extracting Valuable Compounds from Mitragyna speciosa Leaves. AgriEngineering 2023, 5, 1879-1892. Jintawiwat, R.; Punamorntarakul, N.; Hirunyasiri, R.; Jarupoom, P.; Pankasemsuk, T.; Supasin, S.; Kawee-ai, A. Testing the Efficacy of a Prototype That Combines Ultrasound and Pulsed Electric Field for Extracting Valuable Compounds from Mitragyna speciosa Leaves. AgriEngineering 2023, 5, 1879-1892.

Abstract

The aim of this work was to determine the potential of using a pulsed electric field (PEF) and ultra-sound (US) apparatus to produce mitragynine extracts from Mitragyna speciosa dried leaves. Four modes of the device were tested: PEF, US, US + PEF, and PEF + US. The results were compared with extracts obtained using a conventional technique (maceration, as the control). Changes in the mitragynine content were determined with the liquid chromatography/mass spectrometry (LC-MS/MS) method. The LC-MS/MS analysis showed that the mitragynine contents from kratom extracts using four different modes were different. The highest extraction (106.63 ± 0.85 mg/L) of mitragynine was achieved by the PEF + US procedure, followed by US + PEF (97.27 ± 1.33 mg/L), with increased extraction efficiencies of 45.81 ± 0.59% and 33.00 ± 1.85%, respectively. Moreover, the total energy consumption under the combination technique was 25.0% lower than that with PEF assistance. Furthermore, scanning electron microscopy (SEM) and Fourier Transform Infrared Spectroscopy (FTIR) provided confirmatory evidence for the extraction of M. speciosa by the prototype. This study confirmed that PEF and US devices can be considered a green alternative method and may contribute to the application of agricultural products.

Keywords

Mitragyna speciosa; mitragynine; novel technology; energy consumption; pulsed electric field; ultrasound extraction

Subject

Engineering, Industrial and Manufacturing Engineering

Comments (0)

We encourage comments and feedback from a broad range of readers. See criteria for comments and our Diversity statement.

Leave a public comment
Send a private comment to the author(s)
* All users must log in before leaving a comment
Views 0
Downloads 0
Comments 0
Metrics 0


×
Alerts
Notify me about updates to this article or when a peer-reviewed version is published.
We use cookies on our website to ensure you get the best experience.
Read more about our cookies here.