Preprint Article Version 1 Preserved in Portico This version is not peer-reviewed

The Assessment of the Transversal Rupture Strength (TRS) and Hardness of WC-Co Specimens Made via Additive Manufacturing and Sinter-HIP

Version 1 : Received: 4 May 2023 / Approved: 4 May 2023 / Online: 4 May 2023 (09:03:20 CEST)

A peer-reviewed article of this Preprint also exists.

Jucan, O.-D.; Gădălean, R.-V.; Chicinaş, H.-F.; Bâlc, N.; Popa, C.-O. The Assessment of the Transversal Rupture Strength (TRS) and Hardness of WC-Co Specimens Made via Additive Manufacturing and Sinter-HIP. Metals 2023, 13, 1051. Jucan, O.-D.; Gădălean, R.-V.; Chicinaş, H.-F.; Bâlc, N.; Popa, C.-O. The Assessment of the Transversal Rupture Strength (TRS) and Hardness of WC-Co Specimens Made via Additive Manufacturing and Sinter-HIP. Metals 2023, 13, 1051.

Abstract

This study is focused on the mechanical properties of WC-Co composites obtained via Selective Laser Sintering using PA12 as a binder. The as-printed samples were thermally debonded, and sintered, first in vacuum, and then sinter-HIPed at 1400oC, using 50 bar Ar, which has led to relative densities up to 66 %. Optical metallographic images show a microstructure consisting of WC, with an average grain size in the range of 1.4 – 2.0 µm, with isolated large grains, in a well-distributed Co matrix. The shrinkage of the samples was 43 %, with no significant shape distortion. The printing direction of the samples has a great impact on the transversal rupture strength (TRS). Nevertheless, the bending strength was low, with a measured maximum of 612 MPa. SEM images of the fracture surface of TRS samples show the presence of defects that constitute the cause of the low measured values. The hardness values position the obtained composites in the range of medium coarse classical cemented carbides. The results were also related to the amount of free Co after sintering, close to the initial one, as assessed by magnetic measurements, indicating a low degree of interaction with PA12 decomposition products.

Keywords

WC-Co composite; Additive Manufacturing; Transversal Rupture Strength

Subject

Chemistry and Materials Science, Ceramics and Composites

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