Preprint Article Version 1 Preserved in Portico This version is not peer-reviewed

Residual Stresses in VT6 (Ti-6Al-4V) Alloy After Shot Peening Evaluated Using X-Ray Diffraction, Laser Speckle Interferometry and GA-Ion FIB-DIC Micro-Ring-Core Milling

Version 1 : Received: 3 March 2022 / Approved: 4 March 2022 / Online: 4 March 2022 (13:34:03 CET)

A peer-reviewed article of this Preprint also exists.

Somov, P.A.; Statnik, E.S.; Kan, Y.; Pisarev, V.S.; Eleonsky, S.I.; Ozherelkov, D.Y.; Salimon, A.I. FIB-DIC Residual Stress Evaluation in Shot Peened VT6 Alloy Validated by X-ray Diffraction and Laser Speckle Interferometry. Nanomaterials 2022, 12, 1235. Somov, P.A.; Statnik, E.S.; Kan, Y.; Pisarev, V.S.; Eleonsky, S.I.; Ozherelkov, D.Y.; Salimon, A.I. FIB-DIC Residual Stress Evaluation in Shot Peened VT6 Alloy Validated by X-ray Diffraction and Laser Speckle Interferometry. Nanomaterials 2022, 12, 1235.

Abstract

Shot peening has become a well-established technique for the introduction of beneficial compressive Residual Stresses (RS) into the near-surface layers of metallic materials for the purpose of preventing or suppressing fatigue crack nucleation and growth. Ti-alloys are widely used to fabricate compressor blades of aeroengines. Titanium blades that may be susceptible to different modes of damage under cyclic loading (high cycle fatigue, fretting fatigue) are often subjected to shot peening to extend their safe operating time. The control and monitoring of residual stresses in titanium blades is of great importance to assure the safety of aeroengines. The techniques for residual stress evaluation include mechanical methods (material removal) as well as physical methods such as X-ray diffraction. Perhaps the most common and practically accessible form of the latter is the method. Conventional laboratory X-ray diffractometers typically probe samples to the depths up to ~20 µm that correspond to 1x...5x the average grain size for typical metals and alloys. The limitations of the method have been identified and reviewed in the literature, motivating the use of other semi-destructive approaches to evaluate the residual stresses in deeper layers and at more sharply defined locations. In the present report we present a case study of the comparison between non-destructive and semi-destructive evaluation techniques, namely the X-ray diffraction method against the mechanical and FIB-DIC ring-core drilling applied to the samples of VT6 (Russian designation of Ti-6Al-4V) titanium alloy after shot peening with 1 mm steel balls. Mechanical drilling of circular holes of ~2 mm diameter with laser speckle interferometry monitoring of strains gives a rough spatial resolution of a few millimeters, while the Korsunsky FIB-DIC method of Ga-ion beam micro-ring core milling within FIB-SEM with Digital Image Correlation (DIC) deformation analysis delivers spatial resolution down to a few micrometers. Good agreement has been found between the X-ray and FIB-DIC estimates of RS variation profiles as a function of depth in shot peened titanium alloy samples. Some advances in the FIB-DIC method are presented and discussed in terms of the acceleration of data acquisition and interpretation.

Keywords

residual stress; VT6 (Ti-6Al-4V); shot peening; X-ray diffraction; speckle interferometry; Ga-ion FIB-DIC

Subject

Engineering, Mechanical Engineering

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