Simple New Method for the Preparation of La(IO3)3 Nanoparticles

Zoulikha Hebboul; Amira Ghozlane; Robin Turnbull; Ali Benghia; Sara Allaoui; Akun Liang; Daniel Errandonea; Amina Touhami; Abdellah Rahmani; Ibn Khaldoun Lefkaier

doi:10.20944/preprints202011.0692.v1

Preprint Article Version 1 Preserved in Portico This version is not peer-reviewed

Version 1 : Received: 26 November 2020 / Approved: 27 November 2020 / Online: 27 November 2020 (13:50:53 CET)

We present a cost- and time-efficient method for the controlled preparation of single phase La(IO3)3 nanoparticles via a simple soft-chemical route which takes a matter of hours, thereby providing an alternative to the common hydrothermal method which takes days. Nanoparticles of pure α-La(IO3)3 and pure δ-La(IO3)3 were synthesised via the new method depending on the source of iodate ions, thereby demonstrating the versatility of the synthesis route. The crystal structure, nanoparticle size-dispersal and chemical composition were characterised via angle- and energy-dispersive powder X-ray diffraction, scanning electron microscopy and Fourier-transform infrared spectroscopy.

Nanoparticles; La(IO3)3; XRD; FTIR; SEM; Non-linear Optics;

Physical Sciences, Acoustics

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Simple New Method for the Preparation of La(IO₃)₃ Nanoparticles

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