Preprint Article Version 1 Preserved in Portico This version is not peer-reviewed

Analytics of Antimony in Natural Water of Nanoparticle Platinum Electrode by Application Square Wave Voltammetry

Version 1 : Received: 4 May 2020 / Approved: 5 May 2020 / Online: 5 May 2020 (11:01:06 CEST)

How to cite: Alkhawaldeh, A. Analytics of Antimony in Natural Water of Nanoparticle Platinum Electrode by Application Square Wave Voltammetry. Preprints 2020, 2020050072. https://doi.org/10.20944/preprints202005.0072.v1 Alkhawaldeh, A. Analytics of Antimony in Natural Water of Nanoparticle Platinum Electrode by Application Square Wave Voltammetry. Preprints 2020, 2020050072. https://doi.org/10.20944/preprints202005.0072.v1

Abstract

This study on the production of a modern natural water electrochemical antimony (II) test include the use of platinum platinum electrode electrodes. Antimony (II) was pre-concentrated on the modified electrode surface and adsorbed to the surface, oxidizing at E = -680 mV. Compared to the platinum electrode, the platinum nanoelectrode exhibited superior performance and, unexpectedly, received a higher electrochemical response. After 25 min of accumulation, time the best-defined anodic peak was obtained with 0.2 mol L-1 KNO3 pH 5.0. Using these parameters, the L-1 Sb 2 + calibration plot was linear over range 1 = 10−8 to 5x10−6 mol. The precision was tested by carrying out eight replicate measurements at a concentration of 2.5x10−5 mol. L-1; the variance coefficient was 2.9%. The method was applied to analyte determination in water samples from the river. Other metal ion attack on Sb's (II) voltammetric response has been studied. In the SEM image, the nanoparticle electrode was clearly observed and characterized by X-ray diffraction and cyclic voltammetry

Keywords

Nanoparticle; Antimony; Platinum Electrode; Square Wave Voltammetry

Subject

Chemistry and Materials Science, Analytical Chemistry

Comments (0)

We encourage comments and feedback from a broad range of readers. See criteria for comments and our Diversity statement.

Leave a public comment
Send a private comment to the author(s)
* All users must log in before leaving a comment
Views 0
Downloads 0
Comments 0
Metrics 0


×
Alerts
Notify me about updates to this article or when a peer-reviewed version is published.
We use cookies on our website to ensure you get the best experience.
Read more about our cookies here.