Preprint Article Version 1 Preserved in Portico This version is not peer-reviewed

The Physicochemical Method Uses Industrial Leftover Hemp Fibre Cellulose to Make Micron-Sized Hemp Powder

Version 1 : Received: 27 December 2023 / Approved: 28 December 2023 / Online: 28 December 2023 (09:57:34 CET)

How to cite: Shamim, S.M.; Huan, Y.; Gan, L.; Zhang, S. The Physicochemical Method Uses Industrial Leftover Hemp Fibre Cellulose to Make Micron-Sized Hemp Powder. Preprints 2023, 2023122166. https://doi.org/10.20944/preprints202312.2166.v1 Shamim, S.M.; Huan, Y.; Gan, L.; Zhang, S. The Physicochemical Method Uses Industrial Leftover Hemp Fibre Cellulose to Make Micron-Sized Hemp Powder. Preprints 2023, 2023122166. https://doi.org/10.20944/preprints202312.2166.v1

Abstract

One of the most widely available and extensively produced varieties of industrial hemp, which generates a substantial amount of consumer-increasing waste in the form of hemp cellulose. In this study, recycling with a compressed and high-speed method that combines crushing and alkali treatment effectively converts leftover hemp fiber into ultrafine powder. SEM (Scanning Electron Microscopy), AFM (Atomic Force Microscope), FTIR (Fourier-transform Infrared Spectroscopy), and XRD (X-ray Diffraction) examined the original morphology of hemp fiber treated with alkali, fiber heated to 200 ℃, and crushed powder. Particle size, crystallinity, fiber surface, and strength increased and decreased. It became apparent that fiber strength decreased and fiber roughness significantly increased after alkali treatment. Fiber increased significantly, and crystallinity decreased after crushing. It was simple and effective for converting the leftover hemp fiber into micron-sized powder. In about 3 to 5 minutes, approximately 1 kg of dry ultrafine powder with a particle size of 10.44 μm was produced. This production method will significantly enhance future industrial applications of waste hemp fiber.

Keywords

leftover hemp fibre recycling process, chemical treatment with cellulose, making a micron-sized powder, average particle size

Subject

Chemistry and Materials Science, Polymers and Plastics

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