2. Description of Experimental Installations
The research was carried out on two experimental installations. The main part of the work was carried out on a large-scale laboratory installation, and preliminary studies were carried out on small-sized samples. First, let's focus on calibration experiments.
A mixture of gypsum and Portland cement in a ratio of 10:1 was used to produce samples both in the main and in preliminary experiments. The samples for preliminary experiments had a diameter of 104 mm and a height of 60 mm. During sample casting, a brass tube with an outer diameter of 12 mm with a plugged end was placed in the sample, simulating a cased borehole. At the sealed end of the tube, in the middle of the height of the sample, there was a hydraulic fracture initiator in the form of a disk with a diameter of 25 mm, made of two layers of brass mesh with a cell size of 0.3 mm, having a hydraulic connection with the brass tube.
The prepared sample was placed between two aluminum disks with piezoelectric transducers made of PZT piezoceramic discs with a diameter of 8 mm and a thickness of 1 mm. The resonant frequency of piezoelectric transducers was approximately 250 kHz. Before assembly, a layer of silicone compound was applied to the surface of the lower base, and a sample was placed on it. After polymerization of the compound, the upper base was treated in the same way. The bases were oriented in such a way that the upper and lower piezoelectric converters were on the same vertical line. The silicone compound ensured no leakage along the upper and lower surfaces of the sample and created a reliable acoustic contact between the sample and piezoelectric transducers.
The experimental installation diagram is shown in
Figure 1. In addition to the elements described above, there were four racks on the lower base, on which induction displacement meters (LVDT sensors) were mounted, the working rod of which was in contact with the outer surface of the upper disk. Since there were vertical recesses on the side surface of the upper base, which included racks, the correct mutual arrangement of the bases was ensured. The hydraulic fracturing fluid was supplied through a channel in the lower base connected with a central tube. When the hydraulic fracture came out on the side surface of the sample, the fluid flowed freely through it. The assembly was placed in a cylindrical vessel, installed in a hydraulic press with a maximum force of 100 kN, and fixed in it. The lower plate of the press was mounted on a ball bearing, providing compensation for the possible non-parallelism of the bases of the installation and the non-parallelism due to uneven opening of the hydraulic fracture. The sample was evacuated, after which a low-viscosity silicone liquid with a viscosity of approximately 5 MPa·s was poured into the sample container and saturated the sample.
A two-channel syringe pumping system was used to carry out hydraulic fracturing, ensure different values of the fracture opening, and maintain a constant pressure in the hydraulic press. One channel of the pumping unit provided hydraulic fracturing and change in the size of the fracture opening. For this purpose, a medium-viscous silicone liquid with a viscosity of about 0.5 Pa·s was used. The other channel of the pump ensures the maintenance of the pressure in the hydraulic press. During the experiments, the relative movements of the upper and lower bases were measured by LVDT sensors and digitized via an interface device to a personal computer, where they were recorded at an interval of about 0.35 s. The discreteness of measuring the displacement value was 0.2 microns.
Two diametrically opposite piezoelectric transducers sent ultrasonic pulses to probe the fracture in the upper disk. The repetition period of the exciting pulses was 20 ms, while the pulses were sent with a delay of 8 ms relative to each other, which made it possible to separate them in time and facilitate the identification of the received signals during processing. All receivers in the lower disk were used to register the pulses, which made it possible to consider the oblique fall of the acoustic wave on the fracture.
After amplification, the received pulses were fed to the input of a four-channel ADC. The sampling rate was 2.5 MHz per channel. The digitized signals were continuously recorded on the hard disk of a personal computer in several sequential files during the entire experiment, which lasted 10 minutes. A low-speed ADC recorded the pressure in the well and in the hydraulic press with a sampling frequency of 100 Hz. The recordings of pressure, ultrasonic pulses and movements were synchronized.
The main experiments were carried out on a triaxial loading unit developed at IDG RAS and described in detail in several publications [
12,
14,
15]. A brief description of the installation is given below.
The installation consists of two horizontal steel discs with a diameter of 750 mm, between which there is a steel ring with a height of 70 mm and an internal diameter of 430 mm. The ring was placed in the groove of the lower base. The discs and the ring form a working chamber with a diameter of 430 mm at a height of 72 mm. There are several holes in the discs and the ring, which are used for mounting piezoelectric acoustic transducer, pressure sensors, and pumping fluids in and out. The scheme of the experimental setup is shown in
Figure 2.
In the main experiment, the same material was used as in the preliminary experiments, consisting of a mixture of 10 parts of gypsum and one part of Portland cement. This mixture was mixed with water (0.65 liters of water per 1 kg of mixture). The permeability of the model material was 1.1·10
-15 m
2. The issues of similarity and adequacy of the model material used and experimental parameters in relation to hydraulic fracturing in the field were considered in [
14,
15].
The surface of the lower base of the installation was covered with a thin layer (0.3...0.5 mm) of silicone compound, which reduced the tangential stresses arising at the lower interface of the sample and the base due to friction. After solidification the compound, the model material was poured into the working volume of the installation with the top cover removed. The filling was carried out in two stages to create an extended oblique fracture in the sample, simulating a natural fracture. First, a wedge-shaped insert made of polymethylmethacrylate with a wedge angle of 40° was installed in the sample. A schematic image of the insert with its main dimensions is shown in
Figure 3. The insert was oriented so that its plane, forming an angle of 40 ° with the horizontal plane, was parallel to the Y axis of the experimental setup. A day later, the insert was removed. Then, the obtained inclined surface was lubricated with a viscous silicone liquid to prevent a sticking. After that, the remaining volume was filled with a second portion of the model mixture. For simplicity, we will call the resulting interface a natural fracture. After solidifying the model material, the sample was dried for 20 days.
When assembling the installation before the experiment, the sample's surface was covered with a rubber membrane, on top of which the upper disc was installed. A small gap of about 2 mm thick remained between the membrane and the disc, the gap was filled with water under a pressure created by the buffer volume of compressed nitrogen, which provided the necessary vertical compressive stress in the sample. Four sealed chambers made of thin sheet copper are mounted on the inner surface of the side ring to set horizontal stresses. The angular length of each chamber is 80°. The inputs of opposite chambers are connected. The necessary pressures in the chambers are set using a pumping unit operating in a constant pressure maintenance mode. In the experiment, only one pair of cameras was used, located along the X-axis of the sample.
Before the sample creation, a brass tube with a diameter of 12 mm was inserted into the central hole of the lower disc simulating a cased borehole. The tube upper end was plugged. In the middle of tube, a slot was made with a rectangular initiator made of two layers of brass mesh with a cell size of 0.3 mm. A height of the initiator was 10 mm and a length 12 mm. The initiator was oriented along the X-axis of the sample towards the existing fracture in the sample. A schematic representation of the sample in the experimental setup is shown in
Figure 4.
Figure 5 shows the positions of ultrasonic transducers, pore pressure measurement points, and lateral loading chambers. Two supplemental wells were located at points P5 and P15, they were used to vacuumize and saturate the sample with a fluid. In the experiment, a low-viscosity organosilicon liquid with a dynamic viscosity of 5 mPa·s and a density of 918 kg/m
3 was used as a pore fluid.
The same pumping system was used as in the calibration experiment to carry out hydraulic fracturing and maintain a given constant pressure in the lateral loading chambers. The fluid was pumped into the central well with a constant flow rate to create a hydraulic fracture. For this purpose, an organosilicon liquid with a dynamic viscosity of 0.2 Pa·s was used. The pressure in the working well and the vertical pressure and pressure in the side chambers were measured using pressure transducers NAT-8252 manufactured by Trafag AG. The identical transducers were used to measure the pore pressure at the points shown in
Figure 5. The signals from the pressure sensors were recorded using two low-speed ADCs with a sampling frequency of 1000 Hz.
For active acoustic monitoring during the opening of both a hydraulic fracture and a natural fracture, the piezoelectric transducers A5 and A6 were used as emitters in the upper disc, the piezoelectric transducers A11, A12, A13 and A15 located at the lower disc served as receivers. The resonant frequency of the piezoelectric transducers was approximately 250 kHz, as in the preliminary experiments. The repetition period of ultrasonic pulses was 100 ms, and the delay between them was set to 2 ms, which, on the one hand, made it possible to avoid overlapping signals from different emitters, and on the other, made it possible to synchronize the entire set of received signals. The system of generation and registration of ultrasonic pulses was the same as in the calibration experiment described above.
Registering the amplitude of the ultrasonic pulses passed through the fracture, it was possible to estimate the value of its opening. At first, individual pulses were extracted from the ADC recording, and the maximums of their amplitudes were found. Then, the found values were normalized by the average value of the pulse record envelopes at the beginning of the recording. Finally, using normalized values, the fracture opening value was calculated based on the results of calibration experiments.