Preprint Article Version 1 Preserved in Portico This version is not peer-reviewed

Microstructural Analysis of Sintered Ti–Al–C Composite Powder Materials

Version 1 : Received: 29 November 2023 / Approved: 29 November 2023 / Online: 29 November 2023 (10:57:06 CET)

A peer-reviewed article of this Preprint also exists.

Kandrotaitė Janutienė, R.; Syzonenko, O.; Mažeika, D.; Gegeckienė, L.; Venytė, I.; Torpakov, A. Microstructure and Phase Composition of Ti-Al-C Materials Obtained by High Voltage Electrical Discharge/Spark Plasma Sintering. Materials 2024, 17, 115. Kandrotaitė Janutienė, R.; Syzonenko, O.; Mažeika, D.; Gegeckienė, L.; Venytė, I.; Torpakov, A. Microstructure and Phase Composition of Ti-Al-C Materials Obtained by High Voltage Electrical Discharge/Spark Plasma Sintering. Materials 2024, 17, 115.

Abstract

This work deals with the analysis of phase composition of sintered Ti-Al-C composite materials under high voltage electrical discharge. The samples of Ti-Al-C powder composites were tested by SEM, Raman spectroscopy and XRD. It was determined that the treatment of the powder by high voltage electrical discharge (HVED) and further sintering at high temperatures using the method of spark plasma sintering (SPS) encourages the formation of the intermetallic reinforcing phases, carbides and different nanocarbon structures like graphene and fullerenes, as well as pure graphite. Intermetallic phases and nanocarbon structures improve mechanical and physical properties of the composites. By using experimental methods mentioned above, the phase composition of Ti-Al-C powder composites obtained at different sintering temperatures was determined.

Keywords

Electron microscopy; Composites; Powder methods; Spark plasma sintering; High voltage electrical discharge; Fullerenes; Intermetallic phase; Graphene

Subject

Engineering, Mechanical Engineering

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