Preprint Article Version 1 Preserved in Portico This version is not peer-reviewed

Enhancing Surface Characteristics and Combustion Behavior of Black Poplar Wood through Varied Impregnation Techniques

Version 1 : Received: 7 October 2023 / Approved: 9 October 2023 / Online: 10 October 2023 (10:54:27 CEST)

A peer-reviewed article of this Preprint also exists.

Beram, A. Enhancing Surface Characteristics and Combustion Behavior of Black Poplar Wood through Varied Impregnation Techniques. Appl. Sci. 2023, 13, 11482. Beram, A. Enhancing Surface Characteristics and Combustion Behavior of Black Poplar Wood through Varied Impregnation Techniques. Appl. Sci. 2023, 13, 11482.

Abstract

The objective of this work was to improve the thermal stability, flame resistance and surface properties of black poplar (Populus nigra L.) wood via different impregnation methods. The impregnation method was employed through two distinct modalities: vacuum impregnation and immersion impregnation. Here, poplar wood was impregnated with calcium oxide solutions (1%, 3% and 5%). Fourier transform infrared spectroscopic analysis revealed a shift in the typical peaks of cellulose, hemicellulose, and lignin depending on the impregnation method and solution ratio. Thermogravimetric analysis and the limiting oxygen index indicated that the samples impregnated with lime solutions exhibited higher thermal stability than the unimpregnated wood. In both impregnation methods caused a decrease water absorption and thickness swelling of the sample groups. Using a scanning electron microscope, the effect of the impregnation process on the structure of the wood was examined. In terms of surface properties, it was determined that the surface roughness value increased. On the contrary, it was observed that the contact angle value also increased. A significant difference emerged between the applied methods. In conclusion, the applied lime minerals are suitable substances to increase flame resistance and thermal stability of black poplar wood.

Keywords

black poplar; thermal stability; wood protection; impregnation, surface properties

Subject

Chemistry and Materials Science, Paper, Wood and Textiles

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