Preprint Article Version 1 Preserved in Portico This version is not peer-reviewed

Preparation, Characterization of Magnetic Chitosan nanoparticles Coated with Fe3O4 Prepared by Ex-situ Co-precipitation Method

Version 1 : Received: 30 August 2023 / Approved: 30 August 2023 / Online: 31 August 2023 (09:45:41 CEST)

How to cite: Meena, H.M.; Kukreti, S.; Jassal, P. Preparation, Characterization of Magnetic Chitosan nanoparticles Coated with Fe3O4 Prepared by Ex-situ Co-precipitation Method. Preprints 2023, 2023082130. https://doi.org/10.20944/preprints202308.2130.v1 Meena, H.M.; Kukreti, S.; Jassal, P. Preparation, Characterization of Magnetic Chitosan nanoparticles Coated with Fe3O4 Prepared by Ex-situ Co-precipitation Method. Preprints 2023, 2023082130. https://doi.org/10.20944/preprints202308.2130.v1

Abstract

The suspension cross-linking technique has been utilized to create the magnetic chitosan nanoparticles, which were then applied to the magnetic carrier method at 80°C. First the FeCl2 and FeCl3 solution co-precipitated and synthesized Fe3O4 for utilization in the formation of magnetic chitosan nanoparticles, it has been characterized by utilizing DLS (Dynamic light scattering), XRD (X-ray diffraction spectrometer), FTIR (Fourier transform infrared spectroscopy), which identified structure, size, FE-SEM (Field Emission Scanning Electron Microscope) and HR-TEM (High-resolution transmission electron microscopy) which identified structure and particle size whereas magnetic behavior of chitosan nanoparticles was determined by VSM (Vibrating sample magnetometer). According to the results collected, the magnetic chitosan nanoparticles have been spherical in form and size ranging from around 250 to 400 nm.

Keywords

Magnetic nanoparticles; chitosan; XRD; FESEM; FTIR; DLS; VSM; Applications

Subject

Chemistry and Materials Science, Nanotechnology

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