Preprint Article Version 1 Preserved in Portico This version is not peer-reviewed

Effects of Different Toothpastes on the Nanomechanical Properties and Chemical Composition of Resin-Modified Glass Ionomer Cement and Composite Resin Restorations

Version 1 : Received: 5 May 2023 / Approved: 9 May 2023 / Online: 9 May 2023 (12:00:38 CEST)

A peer-reviewed article of this Preprint also exists.

Moda, M.D.; Dos Santos, P.H.; Pini, N.I.P.; Furini, L.N.; Briso, A.L.F.; Assmann, A.; Fagundes, T.C. Effects of Different Toothpastes on the Nanomechanical Properties and Chemical Composition of Resin-Modified Glass Ionomer Cement and Composite Resin Restorations. Dent. J. 2023, 11, 173. Moda, M.D.; Dos Santos, P.H.; Pini, N.I.P.; Furini, L.N.; Briso, A.L.F.; Assmann, A.; Fagundes, T.C. Effects of Different Toothpastes on the Nanomechanical Properties and Chemical Composition of Resin-Modified Glass Ionomer Cement and Composite Resin Restorations. Dent. J. 2023, 11, 173.

Abstract

Purpose: This study aimed to evaluate the nanomechanical properties and chemical composition of restorative materials and dental surfaces using different toothpastes. Methods: Enamel (n=60) and dentin (n=60) bovine blocks were obtained and restored using resin-modified glass ionomer cement (RMGIC, n=30) or composite resin (CR, n=30) to form the dentin adjacent to RMGIC (DRMGIC), enamel adjacent to RMGIC (ERMGIC), dentin adjacent to CR (DCR), and enamel adjacent to CR (ECR). After restoration, one hemiface of each specimen was coated with an acid-resistant varnish to create the control (C) and eroded (E) sides (erosion: 5 days, 4 × 2 min/day; 1% citric acid / abrasion: 2 × 15 s followed by immersion on slurries 2 min). Three toothpastes were used: without fluoride (WF; n=10), sodium fluoride (NaF; n=10), and stannous fluoride (SnF2; n=10). The specimens were analyzed for nanohardness (H), elastic modulus (Er), and chemical composition using energy-dispersive X-ray spectroscopy (EDS) and Raman microscopy. Data were analyzed using ANOVA two-way repeated measures and Tukey’s test (α = 0.05). Results: The NaF presented lower values of H for DRMGIC-C, with a statistical difference for WF (p < 0.05). SnF2 resulted in lower Er values for ERMGIC-E and RMGIC-E than WF and NaF (p < 0.05). WF showed lower calcium and phosphorus concentrations for DCR-E than other types of toothpastes (p < 0.05). Only stannous-based toothpaste damaged the elasticity of eroded glass ionomer restorations performed in enamel. Toothpastes with fluoride was capable for maintaining main chemical elements of dentin adjacent to restorative materials under challenge conditions.

Keywords

abrasion; composite resin; erosion; glass ionomer cement; stannous ion

Subject

Public Health and Healthcare, Other

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