Preprint Article Version 1 Preserved in Portico This version is not peer-reviewed

Studies of Post Heat Treatment of L-PBF-Inconel 718: Effects of Hold Time on Microstructure, Annealing Twins and Hardness

Version 1 : Received: 5 January 2021 / Approved: 6 January 2021 / Online: 6 January 2021 (14:57:26 CET)

A peer-reviewed article of this Preprint also exists.

Tucho, W.M.; Hansen, V. Studies of Post-Fabrication Heat Treatment of L-PBF-Inconel 718: Effects of Hold Time on Microstructure, Annealing Twins, and Hardness. Metals 2021, 11, 266. Tucho, W.M.; Hansen, V. Studies of Post-Fabrication Heat Treatment of L-PBF-Inconel 718: Effects of Hold Time on Microstructure, Annealing Twins, and Hardness. Metals 2021, 11, 266.

Abstract

The widely adopted temperature for solid solution heat treatment (ST) for the conventionally fabricated Inconel 718 is 1100 °C for a hold time of 1 h or less. This ST scheme is however not enough to dissolve Laves and annihilate dislocations completely in samples fabricated with Laser metal powder bed fusion (L-PBF) additive manufacturing (AM)-Inconel 718. In spite this, the highest hardness obtained after aging for ST temperatures (970 - 1250 °C) is at 1100 °C/1h [1]. The unreleased residual stresses in the retained lattice defects are potentially affecting other properties of the material. Hence, this work aims to investigate if a longer hold time of ST at 1100 °C will lead to complete recrystallization while maintaining the strength after aging or not. For this study, L-PBF-Inconel 718 samples were ST at 1100 °C at various hold times (1, 3, 6, 9, 16 or 24 h) and aged to study the effects on microstructure and hardness. In addition, a sample was directly aged to study the effects of bypassing ST. The samples (ST and aged) gain hardness by 43 – 49 %, depending on hold time. A high density of annealing twins evolved during 3 h of ST and the quantity only slightly varies for longer ST.

Keywords

L-PBF; Inconel 718; heat treatment; microstructure; hardnes; recrystallization

Subject

Chemistry and Materials Science, Biomaterials

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