Formation of Layered Composite Materials "CeO2–TiAl6V4" for Medical Purpose by the Method of Magnetron Sputtering

Maria A. Sudarchikova; Elena O. Nasakina; Alexander Sergeevich Baikin; Ivan S. Volchkov; Alexandra A. Melnikova; Anna Vladimirovna Mikhailova; Konstantin Yu. Demin; Sergey V. Konushkin; Konstantin V. Sergienko; Mikhail A. Kaplan; Artem D. Gorbenko; Alexey G. Kolmakov; Michail A. Sevostyanov

doi:10.20944/preprints202307.2082.v1

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preprints.org > chemistry and materials science > surfaces, coatings and films > doi: 10.20944/preprints202307.2082.v1

Preprint Article Version 1 Preserved in Portico This version is not peer-reviewed

Formation of Layered Composite Materials "CeO2–TiAl6V4" for Medical Purpose by the Method of Magnetron Sputtering

Maria A. Sudarchikova

^* ,

Elena O. Nasakina

Alexander Sergeevich Baikin

^* ,

Ivan S. Volchkov

Alexandra A. Melnikova

Anna Vladimirovna Mikhailova

Konstantin Yu. Demin

Sergey V. Konushkin

Konstantin V. Sergienko

Mikhail A. Kaplan

Artem D. Gorbenko

Alexey G. Kolmakov

Michail A. Sevostyanov

Version 1 : Received: 30 July 2023 / Approved: 31 July 2023 / Online: 31 July 2023 (10:15:04 CEST)

How to cite: Sudarchikova, M.A.; Nasakina, E.O.; Baikin, A.S.; Volchkov, I.S.; Melnikova, A.A.; Mikhailova, A.V.; Demin, K.Y.; Konushkin, S.V.; Sergienko, K.V.; Kaplan, M.A.; Gorbenko, A.D.; Kolmakov, A.G.; Sevostyanov, M.A. Formation of Layered Composite Materials "CeO2–TiAl6V4" for Medical Purpose by the Method of Magnetron Sputtering. Preprints 2023, 2023072082. https://doi.org/10.20944/preprints202307.2082.v1 Sudarchikova, M.A.; Nasakina, E.O.; Baikin, A.S.; Volchkov, I.S.; Melnikova, A.A.; Mikhailova, A.V.; Demin, K.Y.; Konushkin, S.V.; Sergienko, K.V.; Kaplan, M.A.; Gorbenko, A.D.; Kolmakov, A.G.; Sevostyanov, M.A. Formation of Layered Composite Materials "CeO2–TiAl6V4" for Medical Purpose by the Method of Magnetron Sputtering. Preprints 2023, 2023072082. https://doi.org/10.20944/preprints202307.2082.v1

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MDPI and ACS Style

Sudarchikova, M.A.; Nasakina, E.O.; Baikin, A.S.; Volchkov, I.S.; Melnikova, A.A.; Mikhailova, A.V.; Demin, K.Y.; Konushkin, S.V.; Sergienko, K.V.; Kaplan, M.A.; Gorbenko, A.D.; Kolmakov, A.G.; Sevostyanov, M.A. Formation of Layered Composite Materials "CeO2–TiAl6V4" for Medical Purpose by the Method of Magnetron Sputtering. Preprints 2023, 2023072082. https://doi.org/10.20944/preprints202307.2082.v1

APA Style

Sudarchikova, M.A., Nasakina, E.O., Baikin, A.S., Volchkov, I.S., Melnikova, A.A., Mikhailova, A.V., Demin, K.Y., Konushkin, S.V., Sergienko, K.V., Kaplan, M.A., Gorbenko, A.D., Kolmakov, A.G., & Sevostyanov, M.A. (2023). Formation of Layered Composite Materials "CeO2–TiAl6V4" for Medical Purpose by the Method of Magnetron Sputtering. Preprints. https://doi.org/10.20944/preprints202307.2082.v1

Chicago/Turabian Style

Sudarchikova, M.A., Alexey G. Kolmakov and Michail A. Sevostyanov. 2023 "Formation of Layered Composite Materials "CeO2–TiAl6V4" for Medical Purpose by the Method of Magnetron Sputtering" Preprints. https://doi.org/10.20944/preprints202307.2082.v1

Abstract

Nano- and micro-sized CeO2 surface layers based on titanium alloy TiAl6V4 were obtained by magnetron sputtering with or without subsequent annealing. The structure of the samples was determined using scanning electron microscopy, Auger electron spectroscopy, energy dispersive spectroscopy, and X-ray diffraction. Hardness was measured by sclerometry. A direct linear dependence of the thickness of the surface layers on the deposition time and an extreme dependence, passing through a maximum, on the power are shown. A decrease in hardness with an increase in the thickness of the cerium oxide coating was noted. An increase in surface roughness, delamination and loosening of the surface layer, presumably associated with annealing, were noted. In samples with a surface layer thinner than 715 nm without annealing and 750 nm after annealing, the formation of a sublayer of TiO2, Al2O3, and Ce(VO4) was found, and in annealed samples with a layer length of less than 300 nm, all cerium dioxide reacted with vanadium dioxide to form vanadate.

Keywords

Magnetron sputtering; cerium dioxide; annealing; hardness; surface layer; biocompatibility

Subject

Chemistry and Materials Science, Surfaces, Coatings and Films

Copyright: This is an open access article distributed under the Creative Commons Attribution License which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.

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