Preprint Article Version 1 Preserved in Portico This version is not peer-reviewed

Influence of Pulsed Interference Laser Heating on Crystallization of amorphous Fe77Cu1Si13B9 Ribbons

Version 1 : Received: 2 April 2024 / Approved: 2 April 2024 / Online: 2 April 2024 (13:00:53 CEST)

A peer-reviewed article of this Preprint also exists.

Radziszewska, A.; Czyż, O. Influence of Pulsed Interference Laser Heating on Crystallisation of Amorphous Fe77Cu1Si13B9 Ribbons. Materials 2024, 17, 2060. Radziszewska, A.; Czyż, O. Influence of Pulsed Interference Laser Heating on Crystallisation of Amorphous Fe77Cu1Si13B9 Ribbons. Materials 2024, 17, 2060.

Abstract

The amorphous Fe77Cu1Si13B9 ribbons were treated with pulsed laser interference heating (PLIH). It was confirmed here that the use of the laser heating process allowed for obtaining two-dimensional crystallised micro-areas, periodically distributed (at a distance of 17µm) on the surface of the amorphous ribbons. The correlation between structural changes (SEM, TEM, HRTEM) and the distribution of magnetic field lines of heated amorphous Fe77Cu1Si13B9 (FeCuSiB) ribbons is presented. Particular attention is paid to structure changes in micro-areas where, by controlling the laser interference heating process, partial crystallisation of amorphous alloys and the formation of clusters or single nanocrystallites (α-Fe(Si)) embedded in an amorphous matrix are given. The addition of copper to the FeSiB alloy promoted inhibition of grain growth. Electron holography of micro-areas confirmed shifts of the magnetic field lines in the areas of nanocrystallites, the presence of which in the structure caused magnetisation of the surrounding amorphous matrix.

Keywords

amorphous alloy; pulsed laser interference heating; FeCuSiB ribbons; magnetic field lines; two-dimentional crystallised micro-area

Subject

Chemistry and Materials Science, Materials Science and Technology

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