Preprint Article Version 1 Preserved in Portico This version is not peer-reviewed

Near Net Shape Manufacturing of Sheets from Al-Li-Based Alloy

Version 1 : Received: 25 January 2024 / Approved: 25 January 2024 / Online: 25 January 2024 (10:12:16 CET)

A peer-reviewed article of this Preprint also exists.

Kihoulou, B.; Králík, R.; Bajtošová, L.; Grydin, O.; Stolbchenko, M.; Schaper, M.; Cieslar, M. Near Net Shape Manufacturing of Sheets from Al-Cu-Li-Mg-Sc-Zr Alloy. Materials 2024, 17, 644. Kihoulou, B.; Králík, R.; Bajtošová, L.; Grydin, O.; Stolbchenko, M.; Schaper, M.; Cieslar, M. Near Net Shape Manufacturing of Sheets from Al-Cu-Li-Mg-Sc-Zr Alloy. Materials 2024, 17, 644.

Abstract

Thin twin-roll cast strips from a model Al-Cu-Mg-Li-Zr alloy with a small addition of Sc were prepared. A combination of a fast solidification rate and a favorable effect of Sc microalloying impacts the size and distribution of primary phase particles and the dimension of eutectic cells. Small interdendritic spacing in the range of 10-15 um enables substitution of the initial long-term homogenization annealing by a two-step annealing at 300 and 450 °C and a short solution treatment at 530 °C before quenching and the final age-hardening procedure. A dense dispersion of small Al3(Sc,Zr) precipitates intensively inhibiting recrystallization forms during this treatment. Further refining and fragmentation of the structure were performed using constrained groove pressing before the solution treatment. Small pre-straining of quenched specimens and subsequent age-hardening simulating T8 temper were used to promote the formation of a homogeneous distribution of strengthening particles and to suppress preferential heterogeneous precipitation on subgrain and grain boundaries. Microstructural features and microhardness evolution during annealing were critically examined and confronted with microstructural characteristics observed on reference mold cast alloy or alloys without Sc alloying. The proposed treatment represents a model near net shape procedure for manufacturing thicker sheets for the aerospace industry.

Keywords

Al-Cu-Li-Mg-Zr alloys; Sc addition; twin-roll casting; constrained groove pressing; solution treatment; aging; pre-deformation; precipitation

Subject

Engineering, Metallurgy and Metallurgical Engineering

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