Preprint Article Version 1 Preserved in Portico This version is not peer-reviewed

Influence of Gd Element on Structure, Thermal, and Magneto-Dielectric Properties of NiFe2O4 Nanoparticles

Version 1 : Received: 10 May 2023 / Approved: 11 May 2023 / Online: 11 May 2023 (05:01:39 CEST)

How to cite: Machakanti, Y.; Naidu, K.C.B.; Suresh Kumar, N. Influence of Gd Element on Structure, Thermal, and Magneto-Dielectric Properties of NiFe2O4 Nanoparticles. Preprints 2023, 2023050790. https://doi.org/10.20944/preprints202305.0790.v1 Machakanti, Y.; Naidu, K.C.B.; Suresh Kumar, N. Influence of Gd Element on Structure, Thermal, and Magneto-Dielectric Properties of NiFe2O4 Nanoparticles. Preprints 2023, 2023050790. https://doi.org/10.20944/preprints202305.0790.v1

Abstract

Ni1-xGdxFe2O4 (x=0.02, 0.04, 0.06 & 0.08) (NGF) nanoparticles were synthesized via hydrothermal method. The X-ray diffraction study confirmed the single-phase cubic spinel structure. The morphology indicated the stones (approximately nanocubes) like structures in the FESEM images. The mass loss, and thermal transition temperatures were evaluated as a function of Gd-content using TG-DTG, and TG-DSC measurements. The M-H loops evidenced the high magnetization values for NGFO as compared to pure nickel ferrite. Cation distribution showed the preferred occupancy of cations in the magnetic spinel system. Frequency dependence of dielectric, conductivity, and impedance parameters was elucidated with increase in Gd-content.

Keywords

Nanoparticles; Ferrites; Hydrothermal; Microscopy; Magnetic; Dielectric

Subject

Chemistry and Materials Science, Ceramics and Composites

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