In this paper, a new process of recovering Ti from vanadic titanomagnetite by beneficiation and metallurgy was conducted. Vanadic titanomagnetite concentrate was treated by carbothermic reduction procedure aimed at producing metallized pellet. Melting can realize separating metallic iron from slag under appropriate level of condition. Ti was mainly existed as the form of anosovite phase (MgTi2O5), through slow cooling, particles of anosovite crystal grow and can be separated by flotation. With the adopting of various analytical techniques, such as chemical analysis, X-ray diffraction (XRD), scanning-electron microscope (SEM) and energy dispersive system (EDS) to determine reduction process, phase transformation, microstructure of slag. Results showed that the degree of metallization can reach up to 94% at conditions of reduction temperature 1250 °C, holding 30 min, then melting 60min to obtain metallic iron and titanium slag. After melting, slow cooling promote at appropriate cooling rate of 5 °C/min, anosovite crystal growth and becomes bigger. Through grinding and flotation separation, an anosovite concentrate containing 72.35% TiO2 with 86.32% was obtained.
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